[1]周锋,万欣,傅迎庆.氧化石墨还原法制备石墨烯及其吸附性能[J].深圳大学学报理工版,2011,28(No.5(377-470)):436-439.
　ZHOU Feng,WAN Xin,and FU Ying-qing.Synthesis and adsorption properties of graphene by reduction of graphite oxide[J].Journal of Shenzhen University Science and Engineering,2011,28(No.5(377-470)):436-439.
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氧化石墨还原法制备石墨烯及其吸附性能()
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《深圳大学学报理工版》[ISSN:1000-2618/CN:44-1401/N]

卷:
第28卷
期数:
2011年No.5(377-470)
页码:
436-439
栏目:
材料科学
出版日期:
2011-09-20

文章信息/Info

Title:
Synthesis and adsorption properties of graphene by reduction of graphite oxide
文章编号:
1000-2618(2011)05-0436-04
作者:
周锋1; 2; 万欣1; 傅迎庆1
1)大连海事大学材料科学与工程系，辽宁大连 116026
2) 清华大学化学系，北京 100084
Author(s):
ZHOU Feng1; 2; WAN Xin1;  and FU Ying-qing1
1)Department of Materials Science and Engineering, Dalian Maritime University, Liaoning Province, Dalian 116026, P．R．China
2)Department of Chemistry, Tsinghua University, Beijing 100084, P．R．China
关键词:
材料科学; 石墨烯; 氧化石墨; 还原法; 染料; 吸附性能
Keywords:
materials science; graphene; graphite oxide; reduction; dye; adsorption
分类号:
TQ 127.1
文献标志码:
A
摘要:
利用液相化学氧化法制备氧化石墨，通过水合肼还原氧化石墨制备石墨烯．采用X射线衍射分析、激光拉曼光谱和透射电子显微镜等测试方法，对石墨烯材料的结构和吸附性能进行分析表征.结果表明，通过氧化石墨还原法制得的石墨烯晶体结构完整性有所降低；石墨烯对极性较大的有机染料亚甲基蓝、甲基橙和罗丹明B的吸附率都在95%以上，对极性较小的有机污染物苯酚和氯苯酚的吸附能力较弱.
Abstract:
The graphite oxide (GO) was prepared by oxiding purified natural graphite via Hummer’s method, and graphene was obtained by reduction of graphite oxide prepared．The structure of graphene was analyzed and characterized by X-ray diffraction analysis (XRD)，laser Raman spectroscopy (LRS) and transmission electron microscopy(TEM)．The most intense feature is the G peak at 1580 cm-1 in the Raman spectrum of graphene，corresponding to the first-order scattering of E2g mode．And there is also a D peak near 1350 cm-1 possibly due to the extensive oxidation．The adsorption experimental results showed the desirable adsorption ability of graphene on the methylene blue，methyl orange and rhodamineB，and adsorption rates were above 95%．The adsorption experiment indicated the absorption capacity of graphene on phenol and chlorophenol was weak．

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备注/Memo

备注/Memo:
收稿日期：2010-11-25；修回日期：2011-03-24
基金项目：国家自然科学基金资助项目（20925725）；中央高校基本科研业务费专项资金资助项目（2011QN138）
作者简介：周锋（1976-），男（汉族），江苏省徐州市人，大连海事大学副教授、博士．E-mail：zhoufeng99@mails.tsinghua.edu.cn
更新日期/Last Update: 2011-09-23