[1]吴玉荷,朱国元,洪耿标,等.薇甘菊化学成分研究[J].深圳大学学报理工版,2007,24(1):102-105.
 WU Yu-he,ZHU Guo-yuan,HONG Geng-biao,et al.Study on the chemical constituents of Mikania micrantha[J].Journal of Shenzhen University Science and Engineering,2007,24(1):102-105.
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薇甘菊化学成分研究()
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《深圳大学学报理工版》[ISSN:1000-2618/CN:44-1401/N]

卷:
第24卷
期数:
2007年1期
页码:
102-105
栏目:
生命科学
出版日期:
2007-01-30

文章信息/Info

Title:
Study on the chemical constituents of Mikania micrantha
文章编号:
1000-2618(2007)01-0102-04
作者:
吴玉荷1朱国元2洪耿标1方宏勋2
1)深圳大学生命科学学院,深圳 518060;
2)香港城市大学深圳研究院,深圳 518057
Author(s):
WU Yu-he1ZHU Guo-yuan2HONG Geng-biao1and FANG Hong-xun2
1)College of Life Science, Shenzhen University,Shenzhen 518060,P.R.China
2)Shenzhen Applied R & D Centres of City University of Hong Kong,Shenzhen 518057,P.R.China
关键词:
薇甘菊化学成分倍半萜黄酮豆甾醇
Keywords:
Mikania micrantha chemical constituents sesquiterpene flavone stigmasterol
分类号:
R 284.1
文献标志码:
A
摘要:
采用硅胶柱色谱分离并结合Sephadex LH-20分离纯化方法,研究薇甘菊(Mikania micrantha H.B.K)地上部分的化学成分,通过理化鉴定和NMR等波谱法进行分析鉴定其化学结构.结果表明,在石油醚部位分离得到2个倍半萜类化合物,结构鉴定为deoxymikanolide (Ⅰ)和dihydromikanolide (Ⅱ);正丁醇部位分离得到3个黄酮类化合物、1个甾醇类化合物和1个有机酸,结构分别鉴定为mikanin(Ⅲ),eupalitin(Ⅳ),豆甾醇-β-D-葡萄糖苷(Ⅴ),3,4′,5,7-tetrahydroxy-6-methoxyflavone 3-O-β-D-glucopyranoside (Ⅵ)和绿原酸(Ⅶ).豆甾醇-β-D-葡萄糖苷和绿原酸为首次从该植物分离得到.
Abstract:
The chemical constituents of Mikania micrantha H.B.K were isolated and purified by using silica-gel column and Sephadex LH-20.The chemical constituents were identified by physicochemical properties and structurally elucidated by NMR spectral analysis. 2 compounds obtained from petroleum ether extract of M. micratha were identified as deoxymikanolide (Ⅰ) and dihydromikanolide (Ⅱ),respectively. 5 compounds obtained from n-butyl alcohol extract were identified as mikanin(Ⅲ),eupalitin(Ⅳ),stigmasterol-β-D-glucoside (Ⅴ),3,4′,5,7-tetrahydroxy-6-methoxyflavone 3-O-β-D-glucopyranoside (Ⅵ) and chlorogenic acid(Ⅶ),respectively. Compounds Ⅴ and Ⅶ were obtained from M. mincrantha for the first time.

参考文献/References:

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备注/Memo

备注/Memo:
收稿日期:2006-02-20;修回日期:2006-10-14
基金项目:广东省自然科学基金资助项目(021295)
作者简介:吴玉荷(1946-),女(汉族),广东省增城市人,深圳大学教授.E-mail:wuyh@szu.edu.cn
更新日期/Last Update: 2007-12-09